Equal-path time-of-flight neutron diffraction

Neutron Time-of-Flight Spectroscopy

The time-of-flight technique is employed in two of the instruments at the NIST Cold Neutron Research Facility (CNRF). A pulsed monochromatic beam strikes the sample, and the energies of scattered neutrons are determined from their times-of-flight to an array of detectors. The time-of-flight method may be used in a variety of types of experiments such as studies of vibrational and magnetic excit...

A Novel Method for Ultrasonic Evaluation of Horizontal Defects Using Time-of-Flight Diffraction

Time-of-flight diffraction method (ToFD) is an amplitude-independent sizing method which is based on the measurement of time-of-flight of defect tip diffracted waves. Although ToFD can measure through-wall length of defect accurately, this method is not capable of measuring horizontal defect size. In this paper, a new ToFD method for evaluating horizontal planar defects is presented. The finite...

Flight Path of Least Time

Glycine zinc sulfate penta­hydrate: redetermination at 10 K from time-of-flight neutron Laue diffraction

Single crystals of glycine zinc sulfate penta-hydrate [systematic name: hexa-aqua-zinc tetra-aquadiglycinezinc bis-(sulfate)], [Zn(H2O)6][Zn(C2H5NO2)2(H2O)4](SO4)2, have been grown by isothermal evaporation from aqueous solution at room temperature and characterized by single-crystal neutron diffraction. The unit cell contains two unique ZnO6 octa-hedra on sites of symmetry -1 and two SO4 tetra...

A Rietveld refinement method for angular- and wavelength-dispersive neutron time-of-flight powder diffraction data

This paper introduces a two-dimensional extension of the well established Rietveld refinement method for modeling neutron time-of-flight powder diffraction data. The novel approach takes into account the variation of two parameters, diffraction angle 2θ and wavelength λ, to optimally adapt to the varying resolution function in diffraction experiments. By doing so, the refinement against angular...